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Coupling of HPLC and chemical reaction detector for the separation and determination of organolead compounds
Summary
Type:
HPLC
Application #:
106730
Catalog#:
720014.40 - MN HPLC Column, Nucleosil C18, 100A, 5um, 4x250mm
Detection:
Fig. 4: chemical reaction detector (Teflon) Fig. 7: chemical reaction detector (glass)
Conditions:
Fig. 4: eluent: 10% MeOH in 0.1μ acetate buffer pH 4.6, flow rate 1ml/min
Fig. 7: eluent: 80% MeOH in 0.1M acetate buffer pH 4.6, flow rate 1ml/min
Authors:
Blaszkewicz; M. et al.
Source:
Z. Anal. Chem. 317 (1984) 221–225
Details
Legend: Fig. 4. Separation of organolead salts, 1.25µg Pb2+, 1µg Me2PbCl2, 1.5µg Me3PbAc, 2µg Et2PbCl2, 3µg Et3PbCl per 250µl mobile phase. Fig. 7. Separation of organotin compounds, 5µg Me3SnCl, 5.2µg Me
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